<p>Rietveld refinement was performed on powder diffraction patterns of a triphasic system, where one phase constitutes an internal standard, to be able to quantify the proportion of product (Ti<sub>3</sub>C<sub>2</sub> MXene) and reactant (Ti<sub>3</sub>AlC<sub>2</sub> MAX phase) present after a synthesis trial. Synthesis trial parameters are determined in a Design of Experiments (DoE) screening design.</p>
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<p>See file 2022-12-06 - Quantitative-Phase-Analysis-QPA-of-MXene-synthesis-product-PXRD-patterns.pdf for full dataset details.</p>
Funding
EPSRC Centre for Doctoral Training in the Science and Technology of Fusion Energy
Engineering and Physical Sciences Research Council