SEM & EDX (Zeiss Sigma) of both dropcast and freeze-cast MXene nanoparticles

Microstructure of freeze-cast (FC) and lyophilised Ti₃C₂T_z aqueous suspensions are imaged with secondary electron microscopy. EDX is deployed on these same samples to verify nanoparticle composition. Dilute Ti₃C₂T_z aqueous suspensions produced from the same synthesis used in the FC structures are dropcast on silicon wafer in an attempt to produce a particle-size distribution with subsequent image analysis.

See attached .pdf for full data and experiment description.